Dioxolane 3 Did you obtain experimental evidence for the for
Dioxolane 3. Did you obtain experimental evidence for the formation of one hydrobenzoin isomer in the reduction reaction with sodium borohydride? Cite evidence and configuration. 2pts
Solution
3. Reduction of benzoin
NaBH4 reduction of benzoin yields dl-pair and meso hydrobenzoin products.
The melting point of meso hydrobenzoin is higher than the melting point of the dl pair of hydrobenzoin. Comparing the melting pointd we obtained from the reaction with the literature, we can identify the isomer formed in the reaction. the color changes from yellow for benzoin to white for the products hydrobenzoin. this confirms that reduction has occured.
